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type="text/css"></style> <div id="ct" class="ct2 wp cl"> <div class="mn"> <div class="bm_haa cl"> <div class="bm_h cl"> <a href="http://www.oecr.com/portal.php?mod=rss&catid=57" class="y xi2 rss" target="_blank" title="RSS">订阅</a><h1 class="xs2">文章</h1> </div></div> <div class="kjkjb"> <div class="bm vw" style="margin-bottom:0;"> <div class="h hm"> <div class="zxtoux"><img src="http://www.oecr.com/uc_server/avatar.php?uid=54876&size=small" /></div> <h1 class="ph">中国科学院西安光机所在等离子体光谱研究领域再次取得重要进展 </h1> <p class="xg1"> 时间：2023-12-26 09:41<a class="zz" href="home.php?mod=space&uid=54876">作者：update</a> 阅读<em id="_viewnum">(424)</em> 评论: <a href="http://www.oecr.com/portal.php?mod=comment&id=9935&idtype=aid" title="查看全部评论"><em id="_commentnum">5</em></a>来自: 西安光机所</p> <div class="zxfb" ><a href="http://www.oecr.com/portal.php?mod=rss&catid=57" class="y xi2 rss" target="_blank" title="RSS">订阅</a></div> </div> <!--[diy=diysummarytop]--><div id="diysummarytop" class="area"></div><!--[/diy]--> <div class="s"> <div class="ss"><div><span>导读： </span>激光诱导击穿光谱技术（LIBS）又称激光诱导等离子体光谱，是一种基于原子发射光谱法的元素分析技术，在多元素分析、实时快速原位检测等方面具有突出优势，并且在痕量物质定性定量分析领域具有重要的应用前景。目前该 ...</div> </div> <!--[diy=diysummarybottom]--><div id="diysummarybottom" class="area"></div><!--[/diy]--> <div class="d"> <!--[diy=diycontenttop]--><div id="diycontenttop" class="area"></div><!--[/diy]--> <table cellpadding="0" cellspacing="0" class="vwtb"><tr><td id="article_content"><p style="box-sizing: border-box; margin: 0px 0px 0.5em; padding: 0px; line-height: 2; font-family: 宋体; font-size: 16px; color: rgb(69, 69, 69); background-color: rgb(255, 255, 255);"> <a href="http://laser.oecr.com" target="_blank" class="relatedlink">激光</a>诱导击穿光谱技术（LIBS）又称激光诱导等离子体光谱，是一种基于原子发射光谱法的元素分析技术，在多元素分析、实时快速原位检测等方面具有突出优势，并且在痕量物质定性定量分析领域具有重要的应用前景。目前该技术已在深空深海探测、地质勘探、生物医药，以及环境监测等众多领域得到广泛应用。但在普遍应用中，LIBS技术面临信号波动大、光谱强度低、信噪比差、探测灵敏度低等不利因素。放电辅助增强策略可实现大幅度的激光等离子体光谱增强，然而，这一方法在液态样品的探测中受液相对放电过程的干扰导致LIBS信号波动大，影响探测光路甚至无法探测，极大阻碍了放电辅助LIBS（DA-LIBS）在液态样品中痕量物种定性或定量分析方面的应用。<o:p style="box-sizing: border-box; margin: 0px; padding: 0px; font-size: 12pt;"></o:p> </p><p style="box-sizing: border-box; margin: 0px 0px 0.5em; padding: 0px; line-height: 2; font-family: 宋体; font-size: 16px; color: rgb(69, 69, 69); background-color: rgb(255, 255, 255);"> 瞬态光学与光子技术国家重点实验室汤洁课题组近年来开展了激光等离子体光谱研究领域的技术攻关。近日，针对放电辅助LIBS在液态样品探测中面临的关键技术性难题，该团队提出了DA-LIBS结合滤纸采样的方法，促进等离子体中更多的物质被持续加热、电离，致使其寿命从几微秒延长至近百微秒，等离子体光谱强度增加1–2个数量级，滤纸均匀采样巧妙克服了液相干扰放电过程及信号稳定性差等不利因素，显著增强激光烧蚀样品的稳定性，等离子体光谱信号稳定性得以提升33%。凭借显著的光谱增强效应，痕量Ca、Ba元素检出限降低至ppb量级（ 1ppb=10-9=十亿分之一），相比于传统单脉冲LIBS，检出限降低近2个数量级。相比于其他LIBS增强技术（如双脉冲LIBS），该方法不仅享有同等高水平的探测灵敏度，还具备低成本、低能耗、装置简易等优势，将在环境与生态废油污染监测中，对污染物质的溯源，以及预防措施的制定，展现出巨大的应用潜力和价值。</p><p style="box-sizing: border-box; margin: 0px 0px 0.5em; padding: 0px; line-height: 2; font-family: 宋体; font-size: 16px; color: rgb(69, 69, 69); background-color: rgb(255, 255, 255);"> <o:p style="box-sizing: border-box; margin: 0px; padding: 0px;"></o:p><a href="http://opt.cas.cn/gb2019/xwzx/tpxw/202312/W020231225428779380259.png" target="_blank" uploadpic="U020231225428491119633.png" oldsrc="W020231225428779380259.png" style="box-sizing: border-box; margin: 0px 0px 0.5em; padding: 0px; background-color: transparent; color: rgb(51, 51, 51); text-decoration: none; transition: all 0.2s ease-in-out 0s; cursor: pointer; line-height: 2; font-size: 12pt;"><img src="http://opt.cas.cn/gb2019/xwzx/tpxw/202312/W020231225428779380259.png" width="600" alt="" oldsrc="W020231225428779380259.png" style="box-sizing: border-box; margin: 0px auto; padding: 0px 0px 10px; border: 0px; vertical-align: middle; display: block; max-width: 100%; height: auto;"></a> </p><p style="box-sizing: border-box; margin: 0px 0px 0.5em; padding: 0px; line-height: 2; font-family: 宋体; font-size: 16px; color: rgb(69, 69, 69); background-color: rgb(255, 255, 255); text-align: center;"> 图 <span lang="EN-US" style="box-sizing: border-box; margin: 0px 0px 0.5em; padding: 0px; line-height: 2; font-size: 12pt;">LIBS</span><span style="box-sizing: border-box; margin: 0px 0px 0.5em; padding: 0px; line-height: 2; font-size: 12pt;">优化原理示意图</span></p><p class="MsoNormal" align="center" style="box-sizing: border-box; margin: 0px 0px 0.5em; padding: 0px; line-height: 24px; font-family: 宋体; font-size: 16px; color: rgb(69, 69, 69); background-color: rgb(255, 255, 255); text-align: center;"> <span lang="EN-US" style="box-sizing: border-box; margin: 0px 0px 0.5em; padding: 0px; line-height: 2; font-size: 12pt;"><o:p style="box-sizing: border-box; margin: 0px; padding: 0px;"></o:p></span></p><p style="box-sizing: border-box; margin: 0px 0px 0.5em; padding: 0px; line-height: 2; font-family: 宋体; font-size: 16px; color: rgb(69, 69, 69); background-color: rgb(255, 255, 255);"> 该项研究成果发表于分析化学领域顶级期刊 Analytical Chemistry（Nature Index 收录，IF：8.0）。此前，研究团队针对固体或粉末检测的放电LIBS技术研究相关成果发布于Cell子刊Cell Reports Physical Science。<o:p style="box-sizing: border-box; margin: 0px; padding: 0px;"></o:p> </p><p style="box-sizing: border-box; margin: 0px 0px 0.5em; padding: 0px; line-height: 2; font-family: 宋体; font-size: 16px; color: rgb(69, 69, 69); background-color: rgb(255, 255, 255);"> 论文第一作者为中国科学院西安光机所博士研究生许博坪，西安光机所是第一完成和通讯单位。该研究工作得到国家自然科学基金、陕西省自然科学基金等项目的大力支持。</p><p style="box-sizing: border-box; margin: 0px 0px 0.5em; padding: 0px; line-height: 2; font-family: 宋体; font-size: 16px; color: rgb(69, 69, 69); background-color: rgb(255, 255, 255);"> 论文链接：https://pubs.acs.org/doi/10.1021/acs.analchem.3c03579 </p><section microsoft="" yahei",="" simsun;="" margin:="" 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class="xg1 xw0">2023-12-26 11:11</span> </dt> <dd>移动客户端还不错。</dd> </dl><a name="comment_anchor_34102"></a> <dl id="comment_34102_li" class="ptm pbm bbda cl"> <dt class="mbm"> <span class="y xw0 xi2"> <a href="javascript:;" onclick="portal_comment_requote(34102, '9935');">引用</a> </span> <a href="http://club.oecr.com/space-uid-38266.html" class="xi2 xw1" c="1">wangjun</a> <span class="xg1 xw0">2023-12-26 10:41</span> </dt> <dd>不错 支持一个了</dd> </dl><a name="comment_anchor_34101"></a> <dl id="comment_34101_li" class="ptm pbm bbda cl"> <dt class="mbm"> <span class="y xw0 xi2"> <a href="javascript:;" onclick="portal_comment_requote(34101, '9935');">引用</a> </span> <a href="http://club.oecr.com/space-uid-65250.html" class="xi2 xw1" c="1">fantao2345</a> <span class="xg1 xw0">2023-12-26 10:11</span> </dt> <dd>沙发？？？</dd> </dl><a name="comment_anchor_34100"></a> <dl id="comment_34100_li" class="ptm pbm bbda cl"> <dt class="mbm"> <span class="y xw0 xi2"> <a href="javascript:;" 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