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<div class="ss"><div><span>导读： </span>近日，中国科学院大连化学物理研究所研究员郭鹏，中国工程院院士、大连化物所研究员刘中民团队，通过精确调控有机结构导向剂，合成了全新的小孔磷铝分子筛DNL-17，并采用三维电子衍射技术，解析了该分子筛复杂的晶体 ...</div> </div> <!--[diy=diysummarybottom]--><div id="diysummarybottom" class="area"></div><!--[/diy]--> <div class="d"> <!--[diy=diycontenttop]--><div id="diycontenttop" class="area"></div><!--[/diy]--> <table cellpadding="0" cellspacing="0" class="vwtb"><tr><td id="article_content"><p style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; font-size: 16px; font-family: 微软雅黑; color: rgb(68, 68, 68); background-color: rgb(255, 255, 255); text-indent: 2em; margin-bottom: 26px !important; line-height: 32px !important;">近日，中国科学院大连化学<a href="http://theory.oecr.com" target="_blank" class="relatedlink">物理</a>研究所研究员<span lang="zh-CN" style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; margin-bottom: 26px !important; line-height: 32px !important;">郭鹏，中国工程院院士、大连化物所研究员刘中民团队，通过精确调控有机结构导向剂，合成了全新的小孔磷铝分子筛</span>DNL-17<span lang="zh-CN" style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; margin-bottom: 26px !important; line-height: 32px !important;">，并采用三维<a href="http://electronic.oecr.com" target="_blank" class="relatedlink">电子</a>衍射技术，解析了该分子筛复杂的<a href="http://material.oecr.com" target="_blank" class="relatedlink">晶体</a>结构。</span></p><p style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; font-size: 16px; font-family: 微软雅黑; color: rgb(68, 68, 68); background-color: rgb(255, 255, 255); text-indent: 2em; margin-bottom: 26px !important; line-height: 32px !important;"><span lang="zh-CN" style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; margin-bottom: 26px !important; line-height: 32px !important;">磷铝</span><span lang="zh-CN" style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; margin-bottom: 26px !important; line-height: 32px !important;">分子筛由磷氧四面体和铝氧四面体通过共氧顶点相互连接而成，具有规则孔道或笼状结构的晶态磷铝酸盐<a href="http://material.oecr.com" target="_blank" class="relatedlink">材料</a>。其中，具有三维贯穿孔道的小孔</span>磷铝<span lang="zh-CN" style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; margin-bottom: 26px !important; line-height: 32px !important;">分子筛在气体选择性吸附和能量储存方面具有独特能力而备受关注。目前，合成此类全新三维小孔</span>磷铝<span lang="zh-CN" style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; margin-bottom: 26px !important; line-height: 32px !important;">分子筛面临挑战。一是有机结构导向剂的</span><span lang="zh-CN" style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; margin-bottom: 26px !important; line-height: 32px !important;">导向机制研究缺失；二是</span>磷铝<span lang="zh-CN" style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; margin-bottom: 26px !important; line-height: 32px !important;">分子筛的晶体尺寸通常在微<a href="http://material.oecr.com" target="_blank" class="relatedlink">纳米</a>甚至纳米级别，但传统的单晶</span>X<span lang="zh-CN" style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; margin-bottom: 26px !important; line-height: 32px !important;">射线衍射</span><span lang="zh-CN" style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; margin-bottom: 26px !important; line-height: 32px !important;">方法难以解析分子筛骨架结构和主客体相互作用，在一定程度上阻碍了全新分子筛的探索合成。</span></p><p style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; font-size: 16px; font-family: 微软雅黑; color: rgb(68, 68, 68); background-color: rgb(255, 255, 255); text-indent: 2em; margin-bottom: 26px !important; line-height: 32px !important;"><span lang="zh-CN" style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; margin-bottom: 26px !important; line-height: 32px !important;">该研究选用双头季铵盐作为</span>有机结构导向剂<span lang="zh-CN" style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; margin-bottom: 26px !important; line-height: 32px !important;">，调控其碳链长度和端基尺寸，合成全新的纳米级小孔磷铝分子筛，并命名为</span>DNL-17<span lang="zh-CN" style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; margin-bottom: 26px !important; line-height: 32px !important;">。进一步，研究利用三维电子衍射技术确定了</span>DNL-17<span lang="zh-CN" style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; margin-bottom: 26px !important; line-height: 32px !important;">的复杂晶体结构。研究发现，</span>DNL-17<span lang="zh-CN" style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; margin-bottom: 26px !important; line-height: 32px !important;">属于</span>ABC-6<span lang="zh-CN" style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; margin-bottom: 26px !important; line-height: 32px !important;">家族，具有小孔</span>8×8×8<span lang="zh-CN" style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; margin-bottom: 26px !important; line-height: 32px !important;">元环三维贯穿孔道，其骨架结构包含四种类型的分子筛笼即</span><em style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; margin-bottom: 26px !important; line-height: 32px !important;">d</em><em style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; margin-bottom: 26px !important; line-height: 32px !important;">6</em><em style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; margin-bottom: 26px !important; line-height: 32px !important;">r</em><span lang="zh-CN" style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; margin-bottom: 26px !important; line-height: 32px !important;">、</span><em style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; margin-bottom: 26px !important; line-height: 32px !important;">can</em><span lang="zh-CN" style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; margin-bottom: 26px !important; line-height: 32px !important;">、</span><em style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; margin-bottom: 26px !important; line-height: 32px !important;">eri</em><span lang="zh-CN" style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; margin-bottom: 26px !important; line-height: 32px !important;">和</span><em style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; margin-bottom: 26px !important; line-height: 32px !important;">cha</em>，<span lang="zh-CN" style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; margin-bottom: 26px !important; line-height: 32px !important;">且沿</span>c<span lang="zh-CN" style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; margin-bottom: 26px !important; line-height: 32px !important;">轴方向形成多达</span>24<span lang="zh-CN" style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; margin-bottom: 26px !important; line-height: 32px !important;">层的复杂堆垛序列</span><span lang="zh-CN" style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; margin-bottom: 26px !important; line-height: 32px !important;">。研究结合<a href="http://theory.oecr.com" target="_blank" class="relatedlink">理论</a>计算和固体核磁碳谱表征结果发现，在</span>DNL-17<span lang="zh-CN" style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; margin-bottom: 26px !important; line-height: 32px !important;">合成过程中，</span>有机结构导向剂<span lang="zh-CN" style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; margin-bottom: 26px !important; line-height: 32px !important;">通过不同构象来稳定不同分子筛笼。</span></p><p style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; font-size: 16px; font-family: 微软雅黑; color: rgb(68, 68, 68); background-color: rgb(255, 255, 255); text-indent: 2em; margin-bottom: 26px !important; line-height: 32px !important;"><span lang="zh-CN" style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; margin-bottom: 26px !important; line-height: 32px !important;">上述研究证实了</span>有机结构导向剂<span lang="zh-CN" style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; margin-bottom: 26px !important; line-height: 32px !important;">可以通过不同构象来构建全新磷铝分子筛结构，为新型分子筛设计合成提供了新思路。同时，研究发现，</span>DNL-17<span lang="zh-CN" style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; margin-bottom: 26px !important; line-height: 32px !important;">在正丁烷和异丁烷分离过程中表现出良好的选择吸附性能。</span></p><p style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; font-size: 16px; font-family: 微软雅黑; color: rgb(68, 68, 68); background-color: rgb(255, 255, 255); text-indent: 2em; margin-bottom: 26px !important; line-height: 32px !important;"><span lang="zh-CN" style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; margin-bottom: 26px !important; line-height: 32px !important;">相关研究成果以</span><em style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; margin-bottom: 26px !important; line-height: 32px !important;">DNL-17: A Small-Pore Aluminophosphate in ABC‑6 Family with 24 Stacking Layers Unraveled by Three-Dimensional Electron Diffraction</em><span lang="zh-CN" style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; margin-bottom: 26px !important; line-height: 32px !important;">为题，发表在《美国化学会志》（</span><em style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; margin-bottom: 26px !important; line-height: 32px !important;">JACS</em><span lang="zh-CN" style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; margin-bottom: 26px !important; line-height: 32px !important;">）上。研究工作</span><span lang="zh-CN" style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; margin-bottom: 26px !important; line-height: 32px !important;">得到国家自然科学基金等的支持。</span></p><p style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; font-size: 16px; font-family: 微软雅黑; color: rgb(68, 68, 68); background-color: rgb(255, 255, 255); text-indent: 2em; margin-bottom: 26px !important; line-height: 32px !important;"><a href="https://doi.org/10.1021/jacs.4c18190" target="_blank" _title="null" textvalue="论文链接" needdownload="false" data-needdownload="false" data-needparse="false" style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; outline: none; text-decoration: none; list-style: none; margin-bottom: 26px !important; color: rgb(41, 102, 202) !important; line-height: 32px !important;">论文链接</a>：https://pubs.acs.org/doi/10.1021/jacs.4c18190</p><p style="margin-top: 0px; margin-right: 0px; margin-left: 0px; padding: 0px; border: 0px; list-style: none; font-size: 16px; font-family: 微软雅黑; color: rgb(68, 68, 68); background-color: rgb(255, 255, 255); text-indent: 2em; margin-bottom: 26px !important; line-height: 32px 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